FRB MFP Precursor CAM Outperforms China Industry Standards
Released
Released
Announcement PDF
10 December 2025
1
FIREBIRD MFP PRECURSOR CAM OUTPERFORMS
CHINA INDUSTRY STANDARDS
Highlights
• MFP PCAM produced using Firebird’s proprietary concentrate to cathode process
technology
• Internal and third-party testing confirms improvement over several key
performance parameters for its MFP PCAM versus China industry standards
• More than 150 individual test batches completed, producing~200kg of MFP PCAM
• 30kg of MFP PCAM supplied to a potential downstream customer for LMFP cathode
production, with initial coin-cell testing indicating excellent material performance
• Production of MFP PCAM, CAM and other high purity battery materials is targeted
at Firebird’s Australian Demonstration Plant (ADP) in 2026
• The ADP will deliver a fully integrated commercialisation pathway from manganese
concentrate to LMFP cathode materials tailored to Western markets
Figure 1. LMFP coin cell batteries incorporating Firebird’s proprietary battery materials.
10 December 2025
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Firebird CEO, Mr Ron Mitchell, commented:
“Achieving performance improvement over China industry standards, across multiple
parameters, is a significant technical milestone for Firebird and a strong validation of our
proprietary battery materials production process. The results, supported by both internal and
independent testwork, give us confidence that our MFP precursor can meet the demanding
requirements of LMFP cathode producers. With more than 150 test batches completed, 200
kilograms of material produced and 30 kilograms already in the hands of a potential
downstream customer, we are now focused on translating this technical success into
commercial outcomes as we progress toward commissioning our Australian Demonstration
Plant in 2026.”
Australian-owned Firebird Metals Limited (ASX: FRB, Firebird or the Company) is
pleased to provide the following update.
MFP precursor testing results exceed China industry standards
Most solution-based lithium manganese iron phosphate (LMFP) manufacturing routes
rely on externally sourced electrolytic manganese metal (EMM) or high-purity manganese
sulphate monohydrate (HPMSM). By contrast, Firebird leverages its proprietary HPMSM
production technology to utilise HPMSM solution prior to crystallisation to produce MFP
precursor (PCAM).
This approach delivers several advantages:
• Lower raw-material costs
• Removal of the crystallisation step, reducing CapEx and OpEx
• Improved process efficiency, with fewer unit operations
• Enhanced control over precursor quality
Using HPMSM directly in solution also enables more precise atomic-level Mn:Fe ratio
control during co-precipitation. This results in superior MFP consistency and produces a
higher-quality precursor and final LMFP cathode material.
From a commercialisation standpoint, the process is readily scalable and more closely
aligned with contemporary cathode-manufacturing requirements.
Testwork completed at Firebird’s China laboratory has demonstrated an improvement
over several key performance parameters compared with China national industry
standards and customer requirements (Table 1).
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Table 1. The Company’s precursor LMFP testing results compared with China industry standards
T/CIAPS0029—20231
and customer requirements.
1 1
Tested as per Chinese standard T/CIAPS0029—2023 Appendix C.6 Specific capacity tested at 25 degrees celcius and 4.5 volts.
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Key parameters of MFP PCAM testing
There are several critical process parameters that influence the performance of MFP PCAM.
Through an extensive test program comprising more than 150 individual batch runs and
producing approximately 200kg of MFP PCAM, Firebird has developed specialist know-how
and deep technical expertise in optimising these parameters. This body of work underpins
the Company’s proprietary understanding of MFP precursor production and is
summarised in Table 2.
Table 2. Key technical parameters impacting MFP PCAM performance.
Item Technical significance
PH Levels The precursor particle morphology can be effectively controlled by precisely
adjusting the pH during co-precipitation.
Temperature Mn and Fe elements exhibit a highly uniform distribution within the
precursor particles, while the spatial distribution of P coincides precisely with
that of the metal ions (Mn + Fe), indicating the formation of a stoichiometric
phosphate compound.
Mixing speed The intense turbulence generated by stirring not only effectively suppressed
crystal growth but also promoted secondary nucleation, thereby achieving a
narrow particle size distribution.
MnFe:P ratio Critical to control this ratio for the performance of LMFP
Impurities
removal from
different
sources
Flexible in using a variety of input materials and ability to remove impurities
effectively.
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Figure 2. The Company’s patented precursor MFP reactor vessel.
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MFP Precursor to be manufactured at the ADP
The ADP will be Australia’s first demonstration-scale facility capable of converting
manganese ore into High-Purity Manganese Sulphate Monohydrate (HPMSM) and
subsequently synthesising Manganese Iron Phosphate (MFP) Precursor Cathode Active
Material (PCAM) and Cathode Active Material (CAM) using patented and proprietary
equipment and processing techniques (Fig. 2 and 3).
The integrated flowsheet converts manganese ore to HPMSM and then to MFP PCAM and
CAM. A key innovation of the combined HPMSM/MFP PCAM process is the retention of
manganese sulphate in solution between stages, eliminating the need to crystallise
HPMSM as an intermediate product. This approach:
• reduces energy consumption;
• simplifies material handling;
• lowers capital intensity; and
• improves overall process efficiency.
Figure 3. The ADP production process pathway showing the production of MFP PCAM and CAM.
Successful ADP validation will:
• Establish a training, knowledge-transfer and development hub, building local
capability in HPMSM, precursor and CAM production while supporting customer-
specific R&D. This platform strengthens Firebird’s capacity to independently develop,
refine and patent new technologies within Australia.
• Provide the technical foundation for commercial-scale feasibility studies for a
concentrate-to-cathode process using Oakover ore as the preferred feed source.
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• Enhance customer engagement by supplying Australian-made samples to initiate
qualification programs with Western partners.
• Support progression toward contractual offtake agreements and/or JV
partnerships with reputable tier-one Western counterparties.
• De-risk the pathway to a commercial-scale manganese battery-materials
facility in Australia, ensuring a smoother transition from demonstration to full-
scale production.
This announcement has been authorised for release by the Board of Firebird Metals
Limited.
For further information contact:
Ron Mitchell
CEO
E: ron.mitchell@firebirdmetals.com.au
Ph: +61 407 726 325
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About Firebird Metals Limited (ASX:FRB)
Firebird Metals is an integrated manganese technology company positioned in the EV and
energy‑storage markets.
The Company’s state‑of‑the‑art lab and research facility demonstrate full flow‑sheet
capability, from manganese ore to finished battery active cathode materials. Firebird
pairs downstream processing know‑how with proprietary technologies, including a
high‑efficiency kiln and advanced crystallisation, targeting lower cost and energy use and
enabling near‑term revenue via equipment sales and licensing.
Firebird is advancing an lithium manganese iron phosphate (LMFP) pathway to near‑term
production of high‑purity manganese sulphate and an LMR program for next‑generation
cathodes.
Firebird also holds 234 Mt of manganese resources in Western Australia, led by Oakover
(176.7 Mt at 9.9% Mn, including Indicated 105.8 Mt at 10.1% Mn2
) and Hill 616 (57.5 Mt at
12.2% Mn3
). The Company has the flexibility to source manganese ore through third‑party
suppliers and stockpiles, with mining optionality retained within its broader portfolio.
JORC Compliance Statement
This announcement contains references to Mineral Resource Estimates, which have been
reported in compliance with Listing Rule 5.8 and extracted from previous ASX
announcements as referenced.
The Company confirms that it is not aware of any new information or data that materially
affects the information previously reported and that all material assumptions and
technical parameters underpinning the Mineral Resource Estimates continue to apply
and have not materially changed.
Competent Persons Statement (Metallurgical Test Work)
The information in this report that relates to metallurgical test work results is based on
information reviewed by Mr Phil Dundas, who is a Member of the Australasian Institute
of Mining and Metallurgy. Mr Dundas is an employee of Sedgman Pty Ltd and consultant
to Firebird Metals Limited. Mr Dundas is a qualified chemical engineer and has sufficient
experience which is relevant to the supervision and interpretation of test work activities
undertaken to qualify as a Competent Person as defined by the 2012 Edition of the
Australasian Code for Reporting of Exploration Results, Mineral Resources and Ore
Reserves (the JORC Code, 2012 Edition). Mr Dundas consents to the inclusion in the
announcement of the matters based on the reviewed information in the form and context
in which it appears.
2
See ASX announcement dated 23 March 2023: Indicated Resource of 105.8Mt at 10.1%; Inferred Resource of 70.9Mt at 9.6% for global
Resource of 176.7 Mt at 9.9% Mn.
3
See ASX announcement dated 1 December 2021: Inferred Resource of 57.5 Mt at 12.2% Mn.
10 December 2025
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Appendix A – JORC Table 1
JORC Table 1 Section 1 – Sampling Techniques and Data
Criteria JORC Code explanation Commentary
Sampling
techniques
Nature and quality of sampling (e.g. cut
channels, random chips, or specific
specialised industry standard
measurement tools appropriate to the
minerals under investigation, such as
downhole gamma sondes, or handheld
XRF instruments, etc.). These examples
should not be taken as limiting the
broad meaning of sampling.
Not Applicable.
Materials used to present metallurgical study
results in this announcement were sourced from
commercial third party manufacturers of refined
chemicals.
Include reference to measures taken to
ensure sample representivity and the
appropriate calibration of any
measurement tools or systems used.
Not Applicable. Materials used to present
metallurgical study results in this announcement
were sourced from commercial third party
manufacturers of refined chemicals.
Aspects of the determination of
mineralisation that are Material to the
Public Report. In cases where ‘industry
standard’ work has been done this
would be relatively simple (e.g. ‘reverse
circulation drilling was used to obtain
1 m samples from which 3 kg was
pulverised to produce a 30 g charge for
fire assay’). In other cases more
explanation may be required, such as
where there is coarse gold that has
inherent sampling problems. Unusual
commodities or mineralisation types
(e.g. submarine nodules) may warrant
disclosure of detailed information
Not Applicable. Material used in the studies
presented in this announcement are
commercially available chemical compounds,
sourced from third party suppliers. Primary
Mineralisation was not sampled.
Drilling
techniques
Drill type (e.g. core, reverse circulation,
open-hole hammer, rotary air blast,
auger, Bangka, sonic, etc.) and details
(e.g. core diameter, triple or standard
tube, depth of diamond tails, face-
sampling bit or other type, whether
core is oriented and if so, by what
method, etc.).
Not Applicable. No sampling from drilling is
presented in this announcement.
10 December 2025
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Criteria JORC Code explanation Commentary
Drill sample
recovery
Method of recording and assessing
core and chip sample recoveries and
results assessed.
Not Applicable. No sampling from drilling is
presented in this announcement.
Measures taken to maximise sample
recovery and ensure representative
nature of the samples.
Not Applicable. No sampling from drilling is
presented in this announcement.
Whether a relationship exists between
sample recovery and grade and
whether sample bias may have
occurred due to preferential loss/gain
of fine/coarse material.
Not Applicable. No sampling from drilling is
presented in this announcement.
Logging Whether core and chip samples have
been geologically and geotechnically
logged to a level of detail to support
appropriate Mineral Resource
estimation, mining studies and
metallurgical studies.
Not Applicable. No sampling from drilling is
presented in this announcement.
Whether logging is qualitative or
quantitative in nature. Core (or
costean, channel, etc.) photography.
Not Applicable. No sampling from drilling is
presented in this announcement.
The total length and percentage of the
relevant intersections logged.
Not Applicable. No sampling from drilling is
presented in this announcement.
Subsampling
techniques
and sample
preparation
If core, whether cut or sawn and
whether quarter, half or all core taken.
Not Applicable. No sampling from drilling is
presented in this announcement.
If non-core, whether riffled, tube
sampled, rotary split, etc. and whether
sampled wet or dry.
Not Applicable. No sampling from drilling is
presented in this announcement.
10 December 2025
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Criteria JORC Code explanation Commentary
For all sample types, the nature, quality
and appropriateness of the sample
preparation technique.
Not Applicable. No sampling from drilling is
presented in this announcement.
Quality control procedures adopted for
all subsampling stages to maximise
representivity of samples.
Not Applicable. No sampling from drilling is
presented in this announcement.
Measures taken to ensure that the
sampling is representative of the in-situ
material collected, including for
instance results for field
duplicate/second-half sampling.
Not Applicable. No sampling from drilling is
presented in this announcement.
Whether sample sizes are appropriate
to the grain size of the material being
sampled.
Not Applicable. No sampling from drilling is
presented in this announcement.
Quality of
assay data
and
laboratory
tests
The nature, quality and
appropriateness of the assaying and
laboratory procedures used and
whether the technique is considered
partial or total.
Not Applicable. No analyses of primary samples
from drilling are presented in this
announcement.
For geophysical tools, spectrometers,
handheld XRF instruments, etc., the
parameters used in determining the
analysis including instrument make
and model, reading times, calibrations
factors applied and their derivation,
etc.
Not Applicable. No analyses of primary samples
from drilling are presented in this
announcement.
Nature of quality control procedures
adopted (e.g. standards, blanks,
duplicates, external laboratory checks)
and whether acceptable levels of
accuracy (i.e. lack of bias) and
precision have been established.
Not Applicable. No analyses of primary samples
from drilling are presented in this
announcement.
10 December 2025
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Criteria JORC Code explanation Commentary
Verification
of sampling
and
assaying
The verification of significant
intersections by either independent or
alternative company personnel.
Not Applicable. No analyses of primary samples
from drilling are presented in this
announcement.
The use of twinned holes. Not Applicable. No analyses of primary samples
from drilling are presented in this
announcement.
Documentation of primary data, data
entry procedures, data verification,
data storage (physical and electronic)
protocols.
Not Applicable. No analyses of primary samples
from drilling are presented in this
announcement.
Discuss any adjustment to assay data. Not Applicable. No analyses of primary samples
from drilling are presented in this
announcement.
Location of
data points
Accuracy and quality of surveys used to
locate drillholes (collar and downhole
surveys), trenches, mine workings and
other locations used in Mineral
Resource estimation.
Not Applicable. No analyses of primary samples
from drilling are presented in this
announcement.
Specification of the grid system used. Not Applicable. No drilling or sampling data is
presented in this announcement.
Quality and adequacy of topographic
control.
Not Applicable. No analyses of primary samples
from drilling are presented in this
announcement.
Data
spacing and
distribution
Data spacing for reporting of
Exploration Results.
Not Applicable. Not Reporting Exploration
Results.
Whether the data spacing and
distribution is sufficient to establish the
degree of geological and grade
continuity appropriate for the Mineral
Resource and Ore Reserve estimation
procedure(s) and classifications
applied.
Not Applicable. Not Reporting Exploration
Results.
Whether sample compositing has been
applied.
Not Applicable. Not Reporting Exploration
Results.
10 December 2025
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Criteria JORC Code explanation Commentary
Orientation
of data in
relation to
geological
structure
Whether the orientation of sampling
achieves unbiased sampling of possible
structures and the extent to which this
is known, considering the deposit type.
Not Applicable. Not Reporting Exploration
Results.
If the relationship between the drilling
orientation and the orientation of key
mineralised structures is considered to
have introduced a sampling bias, this
should be assessed and reported if
material.
Not Applicable. Not Reporting Exploration
Results.
Sample
security
The measures taken to ensure sample
security.
Not Applicable. Not Reporting Exploration
Results.
Audits or
reviews
The results of any audits or reviews of
sampling techniques and data.
Not Applicable. Not Reporting Exploration
Results.
JORC 2012 Table 1 Section 2 – Reporting of Exploration Results
Criteria JORC Code explanation Commentary
Mineral
tenement and
land tenure
status
Type, reference name/number, location
and ownership including agreements
or material issues with third parties
such as joint ventures, partnerships,
overriding royalties, native title
interests, historical sites, wilderness or
national park and environmental
settings.
Not Applicable. The work presented in the body
of this announcement is not directly related to
a Mineral Resource or Exploration Project.
The security of the tenure held at the
time of reporting along with any known
impediments to obtaining a licence to
operate in the area.
Not Applicable. The work presented in the body
of this announcement is not directly related to
a Mineral Resource or Exploration Project.
10 December 2025
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Criteria JORC Code explanation Commentary
Exploration
done by other
parties
Acknowledgment and appraisal of
exploration by other parties.
Not Applicable. The work presented in the body
of this announcement is not directly related to
a Mineral Resource or Exploration Project.
Geology Deposit type, geological setting and
style of mineralisation.
Not Applicable. The work presented in the body
of this announcement is not directly related to
a Mineral Resource or Exploration Project.
Drillhole
Information
A summary of all information material
to the understanding of the exploration
results including a tabulation of the
following information for all Material
drillholes:
Easting and northing of the drillhole
collar
Elevation or RL (Reduced Level –
elevation above sea level in metres) of
the drillhole collar
Dip and azimuth of the hole
Downhole length and interception
depth
Hole length.
Not Applicable. Not Reporting Exploration
Results.
If the exclusion of this information is
justified on the basis that the
information is not Material and this
exclusion does not detract from the
understanding of the report, the
Competent Person should clearly
explain why this is the case.
Not Applicable. Not Reporting Exploration
Results.
Data
aggregation
methods
In reporting Exploration Results,
weighting averaging techniques,
maximum and/or minimum grade
truncations (e.g. cutting of high grades)
and cut-off grades are usually Material
and should be stated.
Not Applicable. Not Reporting Exploration
Results.
Where aggregate intercepts
incorporate short lengths of high grade
results and longer lengths of low grade
results, the procedure used for such
aggregation should be stated and
some typical examples of such
aggregations should be shown in
detail.
Not Applicable. Not Reporting Exploration
Results.
The assumptions used for any
reporting of metal equivalent values
should be clearly stated.
Not Applicable. Not Reporting Exploration
Results.
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Criteria JORC Code explanation Commentary
Relationship
between
mineralisation
widths and
intercept
lengths
These relationships are particularly
important in the reporting of
Exploration Results.
Not Applicable. Not Reporting Exploration
Results.
If the geometry of the mineralisation
with respect to the drillhole angle is
known, its nature should be reported.
Not Applicable. Not Reporting Exploration
Results.
If it is not known and only the
downhole lengths are reported, there
should be a clear statement to this
effect (e.g. ‘downhole length, true width
not known’).
Not Applicable. Not Reporting Exploration
Results.
Diagrams Appropriate maps and sections (with
scales) and tabulations of intercepts
should be included for any significant
discovery being reported These should
include, but not be limited to a plan
view of drillhole collar locations and
appropriate sectional views.
Relevant diagrams are included in the body of
this announcement.
Balanced
reporting
Where comprehensive reporting of all
Exploration Results is not practicable,
representative reporting of both low
and high grades and/or widths should
be practiced to avoid misleading
reporting of Exploration Results.
Not Applicable. Not Reporting Exploration
Results.
Other
substantive
exploration
data
Other exploration data, if meaningful
and material, should be reported
including (but not limited to):
geological observations; geophysical
survey results; geochemical survey
results; bulk samples – size and
method of treatment; metallurgical test
results; bulk density, groundwater,
geotechnical and rock characteristics;
potential deleterious or contaminating
substances.
Firebird Metals Limited is conducting proof-of-
concept flowsheet testwork to produce lithium
manganese iron phosphate (LMFP) cathode
active material (CAM) in a new process that
directly integrates the generation of precursor
manganese sulphate into the production of the
manganese-iron phosphate (MFP) pre-cathode
active material (pCAM) production.
This work, and the flowsheet being developed
demonstrates and ability to produce CAM from
commercially purchased, refined chemicals
from third party independent suppliers.
The process requires the following chemicals,
which Firebird have sourced from the listed
suppliers:
Raw Material Company
MnSO4.H2O ISKY Chemicals Co. Ltd
FeSO4.7H2O
Qianjiang Fangyuan
Titanium Industry Co., Ltd
NH4H2PO4 Hubei Ezhong Ecology
NH3.H2O
Hunan Jinniu Chemical Co.,
Ltd.
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Criteria JORC Code explanation Commentary
Li2CO3
Hunan Tiantai Tianrun
Amperex Technology Co.,
Ltd
C6H12O6 Aladdin
Further work The nature and scale of planned
further work (e.g. tests for lateral
extensions or depth extensions or
large-scale step-out drilling).
Not Applicable. Not Reporting Exploration
Results.
Diagrams clearly highlighting the areas
of possible extensions, including the
main geological interpretations and
future drilling areas, provided this
information is not commercially
sensitive.
Not Applicable. Not Reporting Exploration
Results.
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